These videos can help you perform common maintenance procedures for the Agilent 7000 Series Triple Quadrupole GC/MS. As always, Agilent's Technical Support Team is available to answer any questions you may have regarding installation or maintenance of Agilent products.
Before you start any of the tasks below, please review the important safety precautions on pages 15 to 21 in the 7000 Series Operating Manual found on the Instrument Utilities CD that was delivered with your system.
Installing the GC Column
- In the MassHunter software, initiate a vent and wait for the process to complete
- Turn off the MS and wait for the rough pump to turn off (approximately 60 seconds)
- Remove the front window cover
- Open the vent valve
- Lower the analyzer cover
- Open the front analyzer
- Install the column into transfer line
- Close the front analyzer
- Close the vent valve
- Turn on the MS
- Pump down the MS
- Lift the analyzer cover
- Install the front window cover
Replacing the Filaments
- In the MassHunter software, initiate a vent and wait for the process to complete
- Turn off the MS and wait for the rough pump to turn off (approximately 60 seconds)
- Remove the front window cover
- Open the vent valve
- Lower the analyzer cover
- Open the front analyzer
- Remove the source from the analyzer
- Remove the old filaments
- Install the new filaments
- Replace the source in the analyzer
- Close the front analyzer
- Close the vent valve
- Turn on the MS
- Pump down the MS
- Lift the analyzer cover
- Install the front window cover
Cleaning the EI Ion Source
- In the MassHunter software, initiate a vent and wait for the process to complete
- Turn off the MS and wait for the rough pump to turn off (approximately 60 seconds)
- Remove the front window cover
- Open the vent valve
- Lower the analyzer cover
- Open the front analyzer
- Remove the source from the analyzer
- Remove the filaments
- Identify ion source parts
- Source parts that need to be cleaned (also available as a downloadable and printable document, 541 kb)
- Disassemble the EI source
- Clean the EI source
- Sonicate the source parts
- Reassemble the EI source
- Reinstall the filaments
- Replace the source in the analyzer
- Close the front analyzer
- Close the vent valve
- Turn on the MS
- Pump down the MS
- Lift the analyzer cover
- Install the front window cover
Cleaning the CI Ion Source
- In the MassHunter software, initiate a vent and wait for the process to complete
- Turn off the MS and wait for the rough pump to turn off (approximately 60 seconds)
- Remove the front window cover
- Open the vent valve
- Lower the analyzer cover
- Open the front analyzer
- Remove the source from the analyzer
- Remove the filaments
- Source parts that need to be cleaned (pdf, 541 kb)
- Disassemble the CI source
- Clean the CI source
- Sonicate the source parts
- Reassemble the CI source
- Reinstall the filaments
- Replace the source in the analyzer
- Close the front analyzer
- Close the vent valve
- Turn on the MS
- Pump down the MS
- Lift the analyzer cover
- Install the front window cover
Replacing the Detector Electron Multiplier Horn
- In the MassHunter software, initiate a vent and wait for the process to complete
- Turn off the MS and wait for the rough pump to turn off (approximately 60 seconds)
- Remove the front window cover
- Open the vent valve
- Lower the analyzer cover
- Open the rear analyzer
- Remove the horn from the analyzer
- Install the triple-axis detector horn
- Close the rear analyzer
- Close the vent valve
- Turn on the MS
- Pump down the MS
- Lift the analyzer cover
- Install the front window cover
Filling the Calibration Vial
- Remove the front window cover
- Refill and install the calibration vial
- Install the front window cover
Changing the Pump Oil
- In the MassHunter software, initiate a vent and wait for the process to complete
- Turn off the MS and wait for the rough pump to turn off (approximately 60 seconds)
- Remove the front window cover
- Open the vent valve
- Remove the oil plugs on top of the pump
- Remove the drain plug and drain the oil
- Replace the drain plug
- Add oil to the pump
- Replace the oil plugs on top of the pump
- Close the vent valve
- Turn on the MS
- Pump down the MS
- Install the front window cover