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Course Schedule |
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LC Fundamentals - Operating in a Compliant Environment
| $600(USD) |
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R1653A |
One Day |
Workshop |
| $600(CAD) |
| Description: |
The scope of this workshop includes LC fundamentals, instrument “readiness”, analyst responsibility and their linkage to data integrity.
The workshop will cover what to look for prior to initiating an analysis in order to prevent Out-of-specification test results and laboratory deviations
and to ensure data integrity. |
| Outline: |
- I. Introduction
- II. Preventing Deviations
- III. Preventive Maintenance
- A. Impact on day to day operation and data integrity
- IV. Analyst Responsibility
- A. Key Points to Consider Prior to Analysis
- - Test Method
- - Instrument Overview
- - Instrument Readiness
- - Instrument/Method/Calibration Setup
- B. Key Points to Consider During Analysis
- - Equilibration and Injection Carryover
- - System Suitability Requirements
- - Automated Sequences – Unmanned Systems
- C. Key Points to Consider After Analysis
- - Data
- - OOS/Atypical
- - Reprocessing of Data
- - Documentation
- V. HPLC Technical Overview/Relationship to data integrity
- A. Pump
- B. Auto sampler
- C. Variable Wavelength Detector
- D. Diode Array Detector
- E. Electrochemical Detector
- F. Refractive Index Detector
- VI. Breakout Session
- A. Applying Instrument Assessment Techniques
- B. Preventing Unplanned Events/Actions Taken
- - System Suitability Failures
- - Instrument Shutdown
- - Leaks/Blockages
- - Error Messages
- - Evaluation of Chromatograms
- - Open Discussion
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| Prerequisites: |
None. |
| Equipment: |
None. |
| Student Profile: |
All personnel involved in daily instrument operation, laboratory managers, quality assurance/control personnel. |
| Course Calendar: | Alpharetta, GA | October 30, 2008 |
| Alpharetta, GA | December 18, 2008 |
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